This reaction also goes with phosphoric acid
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This reaction also goes with phosphoric acid
If you substitute 85% phosphoric acid instead, how much would be required?
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LordCrackingtonsonI did several times, mixed the oil 1 to 1 with phosphoric acid, heated it until the gas evolution stopped. Unfortunately, I did only a few hydrolysis and did not record.
w2x3f5Did you use glacial acetic acid and phosphoric acid together.. or just equal amounts phenylacetylemalonate and phosphoric acid?
LordCrackingtonsonH3PO4 only
The original synthesis on page 1 calls for 7.5ml concentrated sulphuric acid.
If you substitute 85% phosphoric acid instead, how much would be required?
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I did several times, mixed the oil 1 to 1 with phosphoric acid, heated it until the gas evolution stopped. Unfortunately, I did only a few hydrolysis and did not record.
Did you use glacial acetic acid and phosphoric acid together.. or just equal amounts phenylacetylemalonate and phosphoric acid?